Volume 13, Issue 1 (March 2026)                   J. Food Qual. Hazards Control 2026, 13(1): 16-24 | Back to browse issues page

Ethics code: Not applicable.


XML Print


Download citation:
BibTeX | RIS | EndNote | Medlars | ProCite | Reference Manager | RefWorks
Send citation to:

Adu O, Ogun S, Ogunrinola O, Fajana O, Olaitan S, Akinola O, et al . Quality Changes in Fresh and Recycled Frying Oil in Nigeria. J. Food Qual. Hazards Control 2026; 13 (1) :16-24
URL: http://jfqhc.ssu.ac.ir/article-1-1334-en.html
Department of Biochemistry, Lagos State University, Ojo, Lagos, PMB 0001, LASU Post Office, Ojo, Lagos, Nigeria , oluwatosin.adu@lasu.edu.ng
Abstract:   (59 Views)
Background: Fried food business is common among street vendors in Nigeria, many of whom reuse frying oils repeatedly due to economic constraints and limited regulatory oversight. Repeated use of frying oil results in physical and chemical degradation, which introduces toxic compounds into the food. This work aimed to determine the physicochemical changes occurring in vegetable oils used by roadside food vendors in Morogbo, a rural area of Lagos state, Nigeria.
Methods: The safety and quality of these oils were assessed by analyzing samples collected from three street vendors on the first and fifth days of the week. Physical and chemical parameters- color intensity, viscosity, refractive index, acid value, Free Fatty Acid (FFA) content, iodine value, and peroxide value (PV)- were measured. Additionally, acrylamide and polycyclic aromatic hydrocarbons (PAHs) concentrations were quantified using High Performance Liquid Chromatography (HPLC). Fresh oils from the vendors served as controls. Results were expressed as the mean ± Standard Error of Mean (SEM) and analyzed using one-way analysis of variance (ANOVA) followed by Tukey’s Honestly Significant Difference (HSD) post-hoc test.  Values of p<0.05 were considered statistically significant. Statistical analyses were performed using GraphPad Prism version 10.4.1
Results: There was significant difference (p<0.05) in the refractive index, viscosity, Peroxide Value (PV), and Free Fatty Acid (FFA) content between the control and the recycled oil. However, there was no significant difference in iodine value and color intensity between the fresh and recycled oil. All the oil samples, including the control, had high acrylamide while the recycled oil had elevated concentrations of some Polycyclic Aromatic Hydrocarbons (PAHs) like benzo[a]pyrene.
Conclusion: This study highlights the significant deterioration in the safety and quality of frying oils used by street vendors in the Morogbo rural area of Lagos State.

DOI: 10.18502/jfqhc.13.1.21377
Full-Text [PDF 729 kb]   (35 Downloads)    
Type of Study: Original article | Subject: Special
Received: 25/02/09 | Accepted: 26/02/26 | Published: 26/03/20

References
1. Adani, G., Filippini, T., Wise, L.A., Halldorsson, T.I., Blaha, L. and Vinceti, M. (2020) 'Dietary intake of acrylamide and risk of breast, endometrial, and ovarian cancers: a systematic review and dose–response meta-analysis', Cancer Epidemiology, Biomarkers and Prevention, 29, pp. 1095–1106. Available at: [DOI:10.1158/1055-9965.EPI-19-1628]
2. Adelagun, R.O., Berezi, E.P., Fagbemi, J.O., Igbaro, O.J., Aihkoje, F.E., Ngana, O., Osondu, G. and Garba, M.S. (2023) 'Evaluation of level of rancidity of edible oil in some fried snacks food', Journal of Chemical Society of Nigeria, 48(1). Available at: [DOI:10.46602/jcsn.v48i1.853]
3. Adu, O.B., Fajana, O.O., Ogunrinola, O.O., Okonkwo, U.V., Evuarherhe, P. and Elemo, B.O. (2019) 'Effect of continuous usage on the natural antioxidants of vegetable oils during deep-fat frying', Scientific African, 5, p. e00144. Available at: [DOI:10.1016/J.SCIAF.2019.E00144]
4. Al-Khusaibi, M. and Rahman, M.S. (2021) 'Quality assessment of frying oil degradation'. In: Khan, M.S. and Rahman, M.S. (eds.) Techniques to Measure Food Safety and Quality: Microbial, Chemical, and Sensory, Cham: Springer International Publishing, pp. 329–344. Available at: [DOI:10.1007/ 978-3-030-68636-9_14]
5. American Oil Chemists' Society (AOCS) (1998) Official Methods and Recommended Practices of the AOCS. Champaign: American Oil Chemists' Society. Available at: https://library.aocs.org/ (Accessed: 3 January 2025).
6. Başaran, B. and Turk, H. (2021) 'The influence of consecutive use of different oil types and frying oil in French fries on the acrylamide level', Journal of Food Composition and Analysis, 104, p. 104177. Available at: [DOI:10.1016/J.JFCA.2021.104177]
7. Bekdeşer, B., Esin Çelik, S., Bener, M., Dondurmacıoğlu, F., Yıldırım, E., Nida Yavuz, E. and Apak, R. (2024) 'Determination of primary and secondary oxidation products in vegetable oils with gold nanoparticle based fluorometric turn-on nanosensor: A new total oxidation value', Food Chemistry, 434, p. 137426. Available at: [DOI:10.1016/J.FOODCHEM.2023.137426]
8. Bureau of Indian Standards (2005) Manual of Methods of Analysis of Food, Oil, and Fat. FAD 10: Food and Agriculture Standard IS: 548 (Part 2). New Delhi: Bureau of Indian Standards.
9. Chebet, J., Kinyanjui, T. and Cheplogoi, P.K. (2016) 'Impact of frying on iodine value of vegetable oils before and after deep frying in different types of food in Kenya', Journal of Scientific and Innovative Research, 5(5), pp. 193–196.
10. Codex Alimentarius Commission (1999) Codex Standard for Named Vegetable Oils (Codex Stan 210-1999). Available at: https://www.fao.org/fao-who-codexalimentarius/sh-proxy/en/?lnk=1&url=https%253A%252F%252Fworkspace.fao.org%252Fsites%252Fcodex%252FStandards%252FCXS%2B210-1999%252FCXS_210e.pdf (Accessed: 5 January 2025).
11. Diamante, L.M. and Lan, T. (2014) 'Absolute viscosities of vegetable oils at different temperatures and shear rate range of 64.5 to 4835 s-1', Journal of Food Processing, 2014(1), p. 234583. Available at: [DOI:10.1155/2014/234583]
12. European Food Safety Authority (EFSA) (2008) 'Polycyclic aromatic hydrocarbons in food: Scientific opinion of the panel on contaminants in the food chain', EFSA Journal, 6(8), p. 724. Available at: [DOI:10.2903/j.efsa.2008.724]
13. Ekpe, O.O., Bassey, S.O., Udefa, A.L. and Essien, N.M. (2018) 'Physicochemical properties and fatty acid profile of Irvingia gabonensis (Kuwing) seed oil', International Journal of Food Science and Nutrition, 3(5), pp. 153–156.
14. Emelike, N.J., Ujong, A.E. and Achinewu, S.C. (2020) 'Physicochemical and antioxidant properties of oils used by local fried food vendors in D/line-Port Harcourt, Rivers State', Agriculture and Food Sciences Research, 7(1), pp. 89–96. Available at: [DOI:10.20448/journal.512.2020.71. 89.96]
15. Fekadu, D., Abera, S. and Weldemichael, H. (2024) 'The influences of street food vendor frying equipment on the quality of frying oil', Heliyon, 10(7), p. e28293. Available at: [DOI:10.1016/j.heliyon.2024.e28293]
16. Gilbraith, W.E., Carter, J.C., Adams, K.L., Booksh, K.S. and Ottaway, J.M. (2021) 'Improving prediction of peroxide value of edible oils using regularized regression models', Molecules, 26(23), p. 7281. Available at: [DOI:10.3390/molecules26237281]
17. Ichu, C.B. and Nwakanma, H.O. (2019) 'Comparative study of the physicochemical characterization and quality of edible vegetable oils', International Journal of Research in Informative Science Application and Techniques (IJRISAT), 3(2), pp. 1–9. Available at: [DOI:10.46828/ijrisat.v3i2.56]
18. Idun-Acquah, N., Obeng, G.Y. and Mensah, E. (2016) 'Repetitive use of vegetable cooking oil and effects on physico-chemical properties – Case of frying with redfish (Lutjanus fulgens)', Science and Technology, 6(1), pp. 8–14. Available at: [DOI:10.5923/j.scit.20160601.02]
19. Ingenbleek, L., Veyrand, B., Adegboye, A., Hossou, S.E., Koné, A.Z., Oyedele, A.D., Kisito, C.S., Dembélé, Y.K., Eyangoh, S. and Verger, P. (2019) 'Polycyclic aromatic hydrocarbons in foods from the first regional total diet study in Sub-Saharan Africa: Contamination profile and occurrence data', Food Control, 103, pp. 133–144. Available at: [DOI:10.1016/j.foodcont.2019.04.006]
20. Indian Standards Institution (ISI) (1984) 'Unsaponifiable matter, RI, Specific gravity, Colour, IV, SV'. In: Handbook of Food Analysis (Part XIII), pp. 62–90. Indian Institution of Standards.
21. ISO 15753 (2006) Animal and Vegetable Fats and Oils – Determination of Polycyclic Aromatic Hydrocarbons. Available at: https://www.iso.org/standard/36703.html (Accessed: 3 January 2025).
22. Kaleem, A., Aziz, S. and Iqtedar, M. (2015) 'Investigating changes and effect of peroxide values in cooking oils subject to light and heat', FUUAST Journal of Biology, 5(2), pp. 191–196.
23. Kalia, J. and Mishra, M. (2019) 'Quality and safety of the frying oils used in small-or medium-sized food enterprises', International Journal of Engineering, Management, Humanities and Social Sciences Paradigms, 31.
24. Karimi, S., Wawire, M. and Mathooko, F.M. (2017) 'Impact of frying practices and frying conditions on the quality and safety of frying oils used by street vendors and restaurants in Nairobi, Kenya', Journal of Food Composition and Analysis, 62, pp. 239–244. Available at: [DOI:10.1016/J.JFCA.2017.07.004]
25. Kostopolou, M., Mylona, A., Nikolaou, A., Lofrano, G., Meric, S. and Belgiorno, V. (2007) 'Determination of polycyclic aromatic hydrocarbons in the harbour sediments of Mytilene, Greece'. In: Proceedings of 10th International Conference on Environmental Science and Technology, pp. A723–A729.
26. Li, G., Wu, S., Wang, L. and Akoh, C.C. (2016) 'Concentration, dietary exposure and health risk estimation of polycyclic aromatic hydrocarbons (PAHs) in youtiao, a Chinese traditional fried food', Food Control, 59, pp. 328–336. Available at: [DOI:10.1016/J.FOODCONT.2015.06.003]
27. Liu, Y., Li, J., Cheng, Y. and Liu, Y. (2019) 'Effect of frying oils' fatty acid profile on quality, free radical and volatiles over deep-frying process: A comparative study using chemometrics', LWT, 101, pp. 331–341. Available at: [DOI:10.1016/j.lwt.2018.11.033]
28. Liu, Z., Tse, L.A., Ho, S.C., Wu, S., Chen, B., Chan, D. and Wong, S.Y. (2017) 'Dietary acrylamide exposure was associated with increased cancer mortality in Chinese elderly men and women: a 11-year prospective study of Mr. and Ms. OS Hong Kong', Journal of Cancer Research and Clinical Oncology, 143, pp. 2317–2326. Available at: [DOI:10.1007/s00432-017-2477-4]
29. Manzoor, S., Masoodi, F.A., Rashid, R., Ahmad, M. and Kousar, M. (2022) 'Quality assessment and degradative changes of deep-fried oils in street fried food chain of Kashmir, India', Food Control, 141, p. 109184. Available at: [DOI:10.1016/j.foodcont.2022.109184]
30. Mariana, R.R., Susanti, E., Hidayati, L. and Wahab, R.A. (2020) 'Analysis of peroxide value, free fatty acid, and water content changes in used cooking oil from street vendors in Malang'. In: AIP Conference Proceedings, 2231. Available at: [DOI:10.1063/5.0002656]
31. Nayak, P.K., Dash, U.M.A., Rayaguru, K. and Krishnan, K.R. (2016) 'Physio-chemical changes during repeated frying of cooked oil: A Review', Journal of Food Biochemistry, 40(3), pp. 371–390. Available at: [DOI:10.1111/jfbc.12215]
32. Ngozi, E.O., Giwa, O.H., Adeoye, B.K., Ani, I.F., Ajuzie, N.C. and Olutayo, T.I. (2019) 'Quality effect of repetitive use of frying oil by street food vendors on quality of the oil', Nigerian Journal of Nutritional Sciences, 40(1), pp. 73–78. Available at: [DOI:10.4314/njns.v40i1]
33. Nova Analytics (2008) Abbe 60 Refractometer User Guide (Issue 4B). Available at: https://img.daihan-sci.com/allforlab/pdf/ Refractometer_Abbe60_man_en.pdf (Accessed: 3 January 2025).
34. Oke, E.K., Idowu, M.A., Sobukola, O.P., Adeyeye, S.A.O. and Akinsola, A.O. (2018) 'Frying of food: a critical review', Journal of Culinary Science and Technology, 16(2), pp. 107–127. Available at: [DOI:10.1080/15428052.2017.1333936]
35. Oladunjoye, O.M. and Aluko, O.O. (2024) 'The perception of food vendors on the associated effects of used cooking oil in Lagos State, Nigeria', International Journal of Environmental Health Research, pp. 1–14. Available at: [DOI:10.1080/09603123.2024.2338888]
36. Pambou-Tobi, N.P., Nzikou, J.M., Matos, L., Ndangui, C.B., Kimbonguila, A., Abena, A.A., Silou, T., Scher, J. and Desobry, S. (2010) 'Comparative study of stability measurements for two frying oils: soybean oil and refined palm oil', Advance Journal of Food Science and Technology, 2(1), pp. 22–27.
37. Phiri, G., Mumba, P. and Mangwera, A. (2006) 'The quality of cooking oil used in informal food processing in Malawi: a preliminary study', International Journal of Consumer Studies, 30(5), pp. 527–532. Available at: [DOI:10.1111/j.1470-6431.2006.00513.x]
38. Pule, O.B. and Torto, N. (2009) Determination of Acrylamide in Cooking Oil by Agilent Bond Elut QuEChERS Acrylamide Kit and HPLC-DAD. Agilent Technologies.
39. Rani, L., Kumar, M., Kaushik, D., Kaur, J., Kumar, A., Oz, F., Proestos, C. and Oz, E. (2023) 'A review on the frying process: Methods, models and their mechanism and application in the food industry', Food Research International, 172, p. 113176. Available at: [DOI:10.1016/J.FOODRES.2023.113176]
40. Wai, T. (2007) 'Local repeatedly used deep-frying oils are generally safe', International Journal of Science and Medical Education, 1, pp. 55–60.
41. Xin, L., Hu, M., Ma, X., Wu, S., Yoong, J.H., Chen, S., Tarmizi, A.H.A. and Zhang, G. (2022) 'Selection of 12 vegetable oils influences the prevalence of polycyclic aromatic hydrocarbons, fatty acids, tocol homologs and total polar components during deep frying', Journal of Food Composition and Analysis, 114, p. 104840. Available at: [DOI:10.1016/j.jfca.2022.104840]
42. Yılmaz, E. and Aydeniz, B. (2011) 'Quantitative assessment of frying oil quality in fast food restaurants', GIDA: The Journal of Food, 36(3).
43. Zhang, Q., Saleh, A.S., Chen, J. and Shen, Q. (2012) 'Chemical alterations taken place during deep-fat frying based on certain reaction products: A review', Chemistry and Physics of Lipids, 165(6), pp. 662–681. Available at: 10.1016/ j.chemphyslip.2012.07.002 [DOI:10.1016/j.chemphyslip.2012.07.002]

Add your comments about this article : Your username or Email:
CAPTCHA

Rights and permissions
Creative Commons License This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.

© 2026 CC BY-NC 4.0 | Journal of food quality and hazards control

Designed & Developed by : Yektaweb